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Download fileSelective Dissolution Process Featuring a Classification Device for the Removal of Fines in Crystallization: Experiments
journal contribution
posted on 2021-10-25, 16:38 authored by Pietro Binel, Marco MazzottiWith the aim of removing fine particles
from a suspension obtained
by crystallization, a selective dissolution process featuring a hydrocyclone
is compared against a well-established partial dissolution process
with a dedicated experimental campaign, which complements an earlier
theoretical study. For this purpose, 3D printed hydrocyclones, solid–liquid
separation devices, are studied in detail and successfully operated
under conditions viable at the laboratory scale. A model due to Braun
is fitted to the experimental results and validated using a cross
validation strategy, thus providing a valuable tool for process simulation.
The experimental campaign is designed to comparatively assess the
efficacy and efficiency of the two processes under analysis as a function
of their respective operating conditions, finally demonstrating the
superior performance of the selective dissolution process. In particular,
it is shown that while in a standard partial dissolution process 20–40%
of the suspended mass has to be dissolved to remove a reasonable amount
of fines, the proposed process reaches the same goal by dissolving
as little as 3–10%.
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removing fine particlesearlier theoretical studycross validation strategy3d printed hydrocyclonesselective dissolution processproposed process reachesrespective operating conditionsdedicated experimental campaignexperimental campaignprocess simulationconditions viableexperimental resultsvaluable toolvalidated usingtwo processesthus providingsuspension obtainedsuspended masssuperior performancesuccessfully operatedreasonable amountmodel duelaboratory scalefinally demonstratingcomparatively assessclassification device