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Microwave-Assisted Catalyst-Free Transesterification of Triglycerides with 1-Butanol under Supercritical Conditions

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journal contribution
posted on 16.12.2015, 14:32 authored by Jeroen Geuens, Jennifer M. Kremsner, Bernd A. Nebel, Sigurd Schober, Roger A. Dommisse, Martin Mittelbach, Serge Tavernier, C. Oliver Kappe, Bert U. W. Maes
A proof-of-concept study has been made to convert rapeseed oil into fatty acid butyl esters by means of microwave irradiation without using a catalyst. High conversions can be reached when the transesterification of triglycerides with 1-butanol was performed under near-critical or supercritical conditions. Microwave heating is an attractive method to perform high-temperature chemistry since the reaction mixture can be heated up considerably faster under carefully controlled conditions.