om900326g_si_001.pdf (65.46 kB)
A Convenient Quick Synthesis of SnBu2RCl Derivatives
journal contribution
posted on 2009-07-13, 00:00 authored by Nora Carrera, Mónica H. Pérez-Temprano, Ana C. Albéniz, Juan A. Casares, Pablo EspinetA convenient method for the quick preparation of SnBu2RX (Bu = n-Bu) has been developed using microwave irradiation and column chromatography in acidic alumina. The method can be a good alternative particularly for easy and quick preparation of small amounts for test purposes and, in general, for the synthesis of compounds that cannot be purified by fractional distillation due to thermal lability or low volatility.