10.1021/cg070598n.s002
Kevin P. Guiry
Kevin P.
Guiry
Simon J. Coles
Simon J.
Coles
Humphrey A. Moynihan
Humphrey A.
Moynihan
Simon E. Lawrence
Simon E.
Lawrence
Effect of 1-Deoxy-d-lactose upon the Crystallization of d-Lactose
American Chemical Society
2008
crystal structure
Crystallization
additive
crystallization
pattern
powder data
synthesis
formation
analysis
room temperature
2008-11-05 00:00:00
Journal contribution
https://acs.figshare.com/articles/journal_contribution/Effect_of_1_Deoxy_d_lactose_upon_the_Crystallization_of_d_Lactose/2902792
The synthesis and crystal structure of 1-deoxy-d-lactose is described, as is its use as an additive in the crystallization of d-lactose. This has resulted in the formation of αβ-d-lactose for the first time at room temperature. Single-crystal analysis shows differences between this analysis and the structure previously obtained from powder data, particularly in the hydrogen-bonding patterns.