10.1021/cg070598n.s002 Kevin P. Guiry Kevin P. Guiry Simon J. Coles Simon J. Coles Humphrey A. Moynihan Humphrey A. Moynihan Simon E. Lawrence Simon E. Lawrence Effect of 1-Deoxy-d-lactose upon the Crystallization of d-Lactose American Chemical Society 2008 crystal structure Crystallization additive crystallization pattern powder data synthesis formation analysis room temperature 2008-11-05 00:00:00 Journal contribution https://acs.figshare.com/articles/journal_contribution/Effect_of_1_Deoxy_d_lactose_upon_the_Crystallization_of_d_Lactose/2902792 The synthesis and crystal structure of 1-deoxy-d-lactose is described, as is its use as an additive in the crystallization of d-lactose. This has resulted in the formation of αβ-d-lactose for the first time at room temperature. Single-crystal analysis shows differences between this analysis and the structure previously obtained from powder data, particularly in the hydrogen-bonding patterns.