Synthesis of Chiral Dotriacontanaphthalenes: How Many Naphthalene Units Are We Able To Elaborately Connect? SueDaisuke TakaishiKazuto HaradaTakunori KurodaReiko KawabataTakeo TsubakiKazunori 2009 (<i>S</i>,<i>S</i>,<i>S</i>,<i>S</i>,<i>S</i>,<i>S</i>,<i>S</i>,<i>S</i>,<i>S</i>,<i>S</i>,<i>S</i>,<i>S</i>,<i>S</i>,<i>S</i>,<i>S</i>,<i>S</i>,<i>S</i>,<i>S</i>,<i>S</i>,<i>S</i>,<i>S</i>,<i>S</i>,<i>S</i>,<i>S</i>,<i>S</i>,<i>S</i>,<i>S</i>,<i>S</i>,<i>S</i>,<i>S</i>,<i>S</i>)-dotriacontanaphthalenes <b>32A</b>−<b>E</b> alternately possessing butoxy and methoxy side chains were precisely constructed through a bottom-up synthesis, and their absolute configurations and fluorescence quantum yields were determined.